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Beilstein J. Org. Chem. 2017, 13, 2087–2093, doi:10.3762/bjoc.13.206
Graphical Abstract
Figure 1: Structure of the VVIA peptide.
Scheme 1: Synthesis of Boc-VVIA-OBn by the ball-milling approach.
Scheme 2: Synthesis of tetrapeptide Boc-VVIA-OBn in solution.
Scheme 3: Synthesis of TFA·H-VVIA-OH by SPPS.
Figure 2: Comparison of the reaction time of the coupling steps performed in the BM and in solution.